November
30
Lab Day 32: Flooding. Serial Dilutions, Spot Titer
Rationale
10 microliter plate was flooded and had serial dilutions performed up to 10^-8. A spot titer was performed to calculate titer by Monday.
Detailed Procedure
- Add 5 mL of PB to 10 microliters plate from previous lab day.
- The plates was shaken on an incubator for one hour.
- Filtered lysate from flooded plate in two separate 50 mL 0.22 µm filtered conical vial.
- 10 µL of 100 was added with 90 µL of phage buffer to create 10-1 dilution which was vortexed.
- 10 µL of 10-1 was added with 90 µL of phage buffer to create 10-2 dilution which was vortexed.
- 10 µL of 10-2 was added with 90 µL of phage buffer to create 10-3 dilution which was vortexed.
- 10 µL of 10-3 was added with 90 µL of phage buffer to create 10-4 dilution which was vortexed.
- 10 µL of 10-4 was added with 90 µL of phage buffer to create 10-5 dilution which was vortexed.
- 10 µL of 10-5 was added with 90 µL of phage buffer to create 10-6 dilution which was vortexed.
- 10 µL of 10-6 was added with 90 µL of phage buffer to create 10-7 dilution which was vortexed.
- 10 µL of 10-7 was added with 90 µL of phage buffer to create 10-8 dilution which was vortexed.
- 4 mL of LB Broth, 45 µL of CaCl2, and 5 mL of 2X TA were combined into a 15 mL vial.
- Transferred and mixed 4.5 mL of the Top Agar (TA) mixture from the conical vial into control plate labeled “SJ Control 11/30/18.”
- Added 0.5 mL Arthro into remaining 4.5 mL TA mixture and poured onto plate labeled “SJ Spot 11/30/18” which was sectioned off into 8 parts
- Waited 15 mins for both plates to solidify.
- Micropipetted 10 µL of 100, 10-1, 10-2, 10-3 ,10-4 , 10-5 , 10-6 , 10-7 , 10-8 in according sections of the spot test plate.
- Rested into incubator
Conclusion
10 microliter plate was completely lysed, which gives hope that a high titer will be achieved by Monday. Only 5 mL of PB was on the plate since the graduated pipette didn’t have up to 10 mL. By next lab day, a new titer will be calculated and hope to achieve a high titer by then.